NMR Notes and Instructions

Experimental

• Experiment Quick Guide
• Diffusion Ordered Spectroscopy (DOSY)
• Non-Uniform Sampling
• Measuring T1 and T2 relaxation times
• Reaction monitoring
• Solvent suppression
• Variable temperature setup
• BBI probe manual tuning for REM400/NCB400

Processing

• Generating 1D stack plots in Topspin
• Phasing phase-sensitive HSQC spectra

Solid State NMR

• 3.2mm Rotor Packing
• 3.2mm PhoenixNMR Probe Manual

Topspin

• Bruker NMR command quick guide
• Multizg, spooler and iconNMR

Troubleshooting

• Locking issues
• UTL300 troubleshooting guide

Other

• Downloading NMR data from server

Useful Websites and Materials

• Integrated Spectral database System of Organic Compounds
• Online NMR Spectrum Predictor
• University of Ottawa NMR Facility Blog
• Routine NMR Experiments (Topspin)
• Chemical Shift Database
• NMR Periodic Table
• NMR Frequency Map
• CIL NMR Solvent Data Chart
• Fulmer et al. Organometallics 2010, 29, 2176 [Article and Supporting Info]
• What is EPR?
• General Intro to IR Spectroscopy
• General Intro to Polarimetry